One-Dimensional MgO Nanostructures with Various Morphologies Grown by Thermal Evaporation Method under Atmospheric Environment

Nam-Woo Kim; Jin-Su Kim; Geun-Hyoung Lee

doi:10.3740/MRSK.2023.33.7.279

All Issue

2023 Vol.33, Issue 7 Preview Page Next Page

Research Paper

One-Dimensional MgO Nanostructures with Various Morphologies Grown by Thermal Evaporation Method under Atmospheric Environment 대기 분위기에서 열증발법에 의해 성장된 여러 가지 형상의 일차원 MgO 나노구조

27 July 2023. pp. 279-284

PDF XML

Abstract

One-dimensional MgO nanostructures with various morphologies were synthesized by a thermal evaporation method. The synthesis process was carried out in air at atmospheric pressure, which made the process very simple. A mixed powder of magnesium and active carbon was used as the source powder. The morphologies of the MgO nanostructures were changed by varying the growth temperature. When the growth temperature was 700 °C, untapered nanowires with smooth surfaces were grown. As the temperature increased to 850 °C, 1,000 °C and 1,100 °C, tapered nanobelts, tapered nanowires and then knotted nanowires were sequentially observed. X-ray diffraction analysis revealed that the MgO nanostructures had a cubic crystallographic structure. Energy dispersive X-ray analysis showed that the nanostructures were composed of Mg and O elements, indicating high purity MgO nanostructures. Fourier transform infrared spectra peaks showed the characteristic absorption of MgO. No catalyst particles were observed at the tips of the one-dimensional nanostructures, which suggested that the one-dimensional nanostructures were grown in a vapor-solid growth mechanism.

Keywords

magnesium oxide

thermal evaporation

one-dimensional nanostructures

diverse morphologies

air atmosphere

References

E. M. Sulaiman, F. A-H. Mutlak and U. M. Nayef, Opt. Quantum Electron., 54, 744 (2022). 10.1007/s11082-022-04156-y

K. Mageshwari, S. S. Mali, R. Sathyamoorthy and P. S. Patil, Powder Technol., 249, 456 (2013). 10.1016/j.powtec.2013.09.016

B. Mangaalampalli, N. Dumala and P. Grover, Nucleus, 62, 227 (2019). 10.1007/s13237-019-00298-9

K. Krishnamoorthy, J. Y. Moon, H. B. Hyun, S. K. Cho and S.-J. Kim, Mater. Chem., 22, 24610 (2012). 10.1039/c2jm35087d

C. W. Wong, Y. S. Chan, J. Jeevanandam, K. Pal, M. Bechelany, M. A. Elkodous and G. S. El-Sayyad, J. Cluster Sci., 31, 367 (2020). 10.1007/s10876-019-01651-3

L. Zhang, W. Zhu, H. Zhang, S. Bi and Q. Zhang, Advances, 4, 30542 (2014). 10.1039/C4RA03971H

M. Kuang, Y. Shang, G. Yang, B. Liu and B. Yang, Environ. Sci. Pollut. Res., 26, 18825 (2019). 10.1007/s11356-019-05277-w31065979

C. Y. Cao, J. Qu, F. Wei, H. Liu and W. G. Song, ACS Appl. Mater. Interfaces, 4, 4283 (2012). 10.1021/am300972z22812446

C. N. Rao, U. T. Nakate, R. J. Choudhary and S. N. Kale, Appl. Phys. Lett., 103, 151107 (2013). 10.1063/1.4824772

S. Ileda, K. Miura, H. Yamantoo, H. D. Gan, M. Endo, S. Kanai, J. Hayakawa, F. Matsukara and H. Ohno, Nat. Mater., 9, 721 (2010). 10.1038/nmat280420622862

O. B. Koper, I. Lagadic, A. Volodin and K. J. Klabunde, Chem. Mater., 9, 2468 (1997). 10.1021/cm970357a

Q. Yang, J. Sha, L. Wang, J. Wang and D. Yang, Mater. Sci. Eng., C, 26, 1097 (2006). 10.1016/j.msec.2005.09.082

Y. Yan, L. Zhou and Y. Zhang, J. Phys. Chem. C, 112, 19831 (2008). 10.1021/jp806639x

Z. Yan, R. Bao, C. M. Busta and D. B. Chrisey, Nanotechnology, 22, 265610 (2011). 10.1088/0957-4484/22/26/26561021576794

M. S. Mastuli, N. Kamarulzaman, M. A. Nawawi, A. M. Mahat, R. Rusdi and N. Kamarudin, Nanoscale Res. Lett., 21, 134 (2014). 10.1186/1556-276X-9-13424650322PMC4003522

X. Li, W. Xiao, G. He, W. Zheng, N. Yu and M. Tan, Colloids Surf., A, 408, 79 (2012). 10.1016/j.colsurfa.2012.05.034

M. Biswas, E. McGlynn, M. O. Henry, M. McCann and A. Rafferty, J. Appl. Phys., 105, 094306 (2009). 10.1063/1.3121213

Y. Zhang, M. Ma, X. Zhang, B. Wang and R. Liu, J. Alloys Compd., 590, 373 (2014). 10.1016/j.jallcom.2013.12.113

N. M. A. Hadia and H. A. Mohamed, Mater. Sci. Semicond. Process., 29, 238 (2015). 10.1016/j.mssp.2014.03.049

Liang, Y. Shimizu, T. Sasaki, H. Umehara and N. Koshizaki, J. Phys. Chem. B, 108, 9728 (2004). 10.1021/jp037963f

S. Kar and S. Chaudhuri, J. Phys. Chem. B, 110, 4542 (2006). 10.1021/jp056058n16526682

H. V. Sheela, V. Madhusudhanan and G. Krishnan, Nanoscale Adv., 1, 1754 (2019). 10.1039/C9NA00072K36134237PMC9417962

Information

Publisher :Materials Research Society of Korea
Publisher(Ko) :한국재료학회
Journal Title :Korean Journal of Materials Research
Journal Title(Ko) :한국재료학회지
Volume : 33
No :7
Pages :279-284
Received Date : 2023-05-18
Revised Date : 2023-06-12
Accepted Date : 2023-06-29
DOI :https://doi.org/10.3740/MRSK.2023.33.7.279

Korean Journal of Materials Research ISSN:1225-0562(Print) 2287-7258(Online) 한국재료학회지

All Issue