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2025 Vol.35, Issue 2 Preview Page

Research Paper

High-Temperature Oxy-Acetylene Torch Test of Filament-Wound Cf/SiC-ZrB2 Composite Ring

필라멘트 와인딩 공법으로 제작한 Cf/SiC-ZrB2 복합체의 고온 산소-아세틸렌 토치 평가

Yoonjae Cho1*
,
Seung Yong Lee1*
,
Jung Hoon Kong1
,
Sanghyeon Kim1
,
Jae-Hyeong Choi1
,
Do Kyung Kim1†
조 윤재1*
,
이 승용1*
,
공 정훈1
,
김 상현1
,
최 재형1
,
김 도경1†
1Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Daejeon 34141, Republic of Korea
1한국과학기술원 신소재공학과
†Corresponding author E-Mail : dkkim@kaist.ac.kr (D. K. Kim, KAIST)
*These two authors are equally contributed as first authors.
27 February 2025. pp. 107-114
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Abstract

Composites of carbon fiber-reinforced silicon carbide (Cf/SiC) with ultra-high temperature ceramics (UHTCs) exhibit superior resistance to oxidation and ablation under high temperatures. Components in large-scale applications often have complex geometries, making it crucial to understand the oxidation and ablation behaviors of curved and non-uniform surfaces. In this study, a Cf/SiC-ZrB2 composite was fabricated into a 300 mm cylindrical shape using filament winding and liquid silicon infiltration processes. The resulting specimens exhibited a uniform microstructure, with SiC and ZrB2 crystals evenly distributed across the top and bottom surfaces, demonstrating the feasibility of producing large-scale composites. The specimens underwent an oxyacetylene torch test at 2,100 K for 5 min to assess their ablation and oxidation performance. The results revealed significant variation in the oxide layer due to the non-flat surface, with the layer thickness gradually decreasing as the oblique angle was reduced. Additionally, the presence of high-melting-point ZrO2 in the oxide layer near the torch center was attributed to the migration and solidification of molten SiO2. This suggests that large and complex Cf/SiC incorporating UHTCs can effectively form a protective oxide layer, even under conditions where SiO2 displacement occurs. The findings underscore the importance of integrating geometric considerations into the design of ultra-high temperature ceramic composites to achieve the thermal and ablation resistance required for advanced high-temperature applications.

Keywords
Cf/SiC-ZrB2 composite
filament winding
liquid silicon infiltration
oxy-acetylene torch test
non-uniform shape
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Information
  • Publisher :Materials Research Society of Korea
  • Publisher(Ko) :한국재료학회
  • Journal Title :Korean Journal of Materials Research
  • Journal Title(Ko) :한국재료학회지
  • Volume : 35
  • No :2
  • Pages :107-114
  • Received Date : 2025-01-02
  • Revised Date : 2025-01-29
  • Accepted Date : 2025-02-03
  • DOI :https://doi.org/10.3740/MRSK.2025.35.2.107
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