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2020 Vol.30, Issue 11
Pulverization and Densification Behavior of YAG Powder Synthesized by PVA Polymer Solution Method
Hyun-Ho Im1
,
Sang-Jin Lee12†
1Department of Advanced Materials Science and Engineering, Mokpo National University, Muan 534-729, Republic of Korea
2The Research Institute of Ceramic Industry Technology, Mokpo National University, Muan 534-729, Republic of Korea
†Corresponding author E-Mail : lee@mokpo.ac.kr (S.-J. Lee, Mokpo Nat'l Univ.)
October 2020. pp. 573-580
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Abstract

YAG (Yttrium Aluminum Garnet, Y3Al5O12) has excellent plasma resistance and recently has been used as an alternative to Y2O3 as a chamber coating material in the semiconductor process. However, due to the presence of an impurity phase and difficulties in synthesis and densification, many studies on YAG are being conducted. In this study, YAG powder is synthesized by an organic-inorganic complex solution synthesis method using PVA polymer. The PVA solution is added to the sol in which the metal nitrate salts are dissolved, and the precursor is calcined into a porous and soft YAG powder. By controlling the molecular weight and the amount of PVA polymer, the effect on the particle size and particle shape of the synthesized YAG powder is evaluated. The sintering behavior of the YAG powder compact according to PVA type and grinding time is studied through an examination of its microstructure. Single phase YAG is synthesized at relatively low temperature of 1,000 oC and can be pulverized to sub-micron size by ball milling. In addition, sintered YAG with a relative density of about 98 % is obtained by sintering at 1,650 oC.

Keywords
YAG
PVA solution method
synthesis
sintering
microstructure
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Information
  • Publisher :Materials Research Society of Korea
  • Publisher(Ko) :한국재료학회
  • Journal Title :Korean Journal of Materials Research
  • Journal Title(Ko) :한국재료학회지
  • Volume : 30
  • No :11
  • Pages :573-580
  • Received Date : 2020-09-08
  • Revised Date : 2020-09-20
  • Accepted Date : 2020-09-24
  • DOI :https://doi.org/10.3740/MRSK.2020.30.11.573
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