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2021 Vol.31, Issue 6 Preview Page

Technical Report

Failure and Phase Transformation Mechanism of Multi-Layered Nitride Coating for Liquid Metal Injection Casting Mold
Changwoo Jeon1†
,
Juho Lee2
,
Eun Soo Park2†
1School of Engineering, Brown University, Providence, Rhode Island 02912, USA
2Eloi Materials Laboratory, Suwon 16229, Republic of Korea
†Corresponding author E-Mail : changwoo_jeon@brown.edu (C. Jeon, Brown Univ.)
June 2021. pp. 331-338
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Abstract

Ti-Al-Si target and Cr-Si target are sputtered alternately to develop a multi-layered nitride coating on a steel mold to improve die-casting lifetime. Prior to the multi-layer deposition, a CrN layer is developed as a buffer layer on the mold to suppress the diffusion of reactive elements and enhance the cohesive strength of the multi-layer deposition. Approximately 50 nm CrSiN and TiAlSiN layers are deposited layer by layer, and form about three μm-thickness of multi-layered coating. From the observation of the uncoated and coated steel molds after the acceleration experiment of liquid metal injection casting, the uncoated mold is severely eroded by the adhesion of molten metallic glass. On the other hand, the multi-layer coating on the mold prevents element diffusion from the metallic glass and mold erosion during the experiment. The multi-layer structure of the coating transforms the nano-composite structured coating during the acceleration test. Since the nano-composite structure disrupts element diffusion to molten metallic glass, despite microstructure changes, the coating is not eroded by the 1,050 °C molten metallic glass.

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Information
  • Publisher :Materials Research Society of Korea
  • Publisher(Ko) :한국재료학회
  • Journal Title :Korean Journal of Materials Research
  • Journal Title(Ko) :한국재료학회지
  • Volume : 31
  • No :6
  • Pages :331-338
  • Received Date : 2021-04-30
  • Revised Date : 2021-05-18
  • Accepted Date : 2021-05-18
  • DOI :https://doi.org/10.3740/MRSK.2021.31.6.331
Journal Informaiton Korean Journal of Materials Research Korean Journal of Materials Research
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